Multi-elemental characterization of semolina samples by inductively coupled plasma-tandem mass spectrometry (ICP-MS/MS)

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dc.authorid0000-0003-3870-8779en_US
dc.authorid0000-0001-6508-6042en_US
dc.authorid0000-0003-3463-9841en_US
dc.authorid0000-0002-7417-9088en_US
dc.contributor.authorArı, Akif
dc.contributor.authorArı, Pelin Ertürk
dc.contributor.authorErmişer, Dönüş
dc.contributor.authorCındık, Betül
dc.contributor.authorYalçın, Erkan
dc.contributor.authorGaga, Eftade Emine
dc.date.accessioned2023-07-05T06:07:16Z
dc.date.available2023-07-05T06:07:16Z
dc.date.issued2022en_US
dc.departmentBAİBÜ, Mühendislik Fakültesi, Çevre Mühendisliği Bölümüen_US
dc.description.abstractThe precise characterization of the elemental composition of cereals and cereal products is becoming crucial to assess their nutritional values, geographical labeling, and also toxicological profile. Inductively coupled plasma-mass spectrometry (ICP-MS) has become popular for the elemental analysis of foods in recent years. Analytical performance of the inductively coupled plasma-tandem mass spectrometry (ICP-MS/MS) is improved with a reaction/collision cell that provides an interference-free analysis of most of the elements including phosphorus and sulfur. In this study, an analytical method was optimized for the quantification of 57 elements using ICP-MS/MS technique and validated for 25 elements that were available in certified reference materials (CRMs). Then, the mineral contents of semolina samples obtained from the durum wheat (Triticum durum) cultivars were analyzed according to the validation procedure. Recoveries of the elements were found in the range of 92-108% for the digested CRM. The method was robust for all elements and the results indicated good precision for the analytical method. The inter- and intra-day precision values were found below 5%, and in the range of 0.11-3.31% and 0.09-4.51%, respectively. Analyzed elements showed significant variability among the semolina samples. The variety and growing conditions might have influences on the elemental composition of semolina samples.en_US
dc.identifier.citationArı, A., Ertürk Arı, P., Ermişer, D., Cındık, B., Yalçın, E., & Gaga, E. O. (2022). Multi-elemental characterization of semolina samples by inductively coupled plasma-tandem mass spectrometry (ICP-MS/MS). Biological Trace Element Research, 200(7), 3462-3473.en_US
dc.identifier.doi10.1007/s12011-021-02933-6
dc.identifier.endpage3473en_US
dc.identifier.issn0163-4984
dc.identifier.issn1559-0720
dc.identifier.issue7en_US
dc.identifier.pmid34559378en_US
dc.identifier.scopus2-s2.0-85115640493en_US
dc.identifier.scopusqualityQ1en_US
dc.identifier.startpage3462en_US
dc.identifier.urihttp://dx.doi.org/10.1007/s12011-021-02933-6
dc.identifier.urihttps://hdl.handle.net/20.500.12491/11236
dc.identifier.volume200en_US
dc.identifier.wosWOS:000698876300001en_US
dc.identifier.wosqualityQ2en_US
dc.indekslendigikaynakWeb of Scienceen_US
dc.indekslendigikaynakScopusen_US
dc.indekslendigikaynakPubMeden_US
dc.institutionauthorArı, Akif
dc.institutionauthorArı, Pelin Ertürk
dc.institutionauthorYalçın, Erkan
dc.language.isoenen_US
dc.publisherSpringernatureen_US
dc.relation.ispartofBiological Trace Element Researchen_US
dc.relation.publicationcategoryMakale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanıen_US
dc.rightsinfo:eu-repo/semantics/closedAccessen_US
dc.subjectTrace Element Characterizationen_US
dc.subjectMethod Validationen_US
dc.subjectFood Elemental Compositionen_US
dc.subjectSulfuren_US
dc.subjectFooden_US
dc.subjectBiodieselen_US
dc.titleMulti-elemental characterization of semolina samples by inductively coupled plasma-tandem mass spectrometry (ICP-MS/MS)en_US
dc.typeArticleen_US

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