Microwave-assisted synthesis and odor characteristics of some new isoxazolidines

Basit Öğe Kaydı
dc.authorid0000-0003-0759-334Xen_US
dc.contributor.authorSağırlı, Akın
dc.contributor.authorAcar, Havva
dc.contributor.authorÖzçal, Hakan Emre
dc.contributor.authorBüyükbayram, Muhammet
dc.date.accessioned2023-08-04T07:54:41Z
dc.date.available2023-08-04T07:54:41Z
dc.date.issued2022en_US
dc.departmentBAİBÜ, Fen Edebiyat Fakültesi, Kimya Bölümüen_US
dc.descriptionTUBITAK (Turkish Scientific and Technological Research Council)(Turkiye Bilimsel ve Teknolojik Arastirma Kurumu (TUBITAK))en_US
dc.description.abstractWe describe herein the design and synthesis of new isoxazolidin-5-carboxylates by microwave-assisted 1,3-dipolar cycloadditions of aldonitrones, derived from five fragrant aldehydes, with methacrylate esters. The reaction proceeded regioselectively providing mostly endo- diastereomers and in some cases an inseparable mixture of endo-exo products. The structures of target compounds were identified on the basis of IR, NMR, and TOF-MS measurements. Besides, both aldonitrone and isoxazolidine derivatives were subjected to olfactory evaluation by an expert nose. Diverse fragrance notes were observed in each series of isoxazolidines bearing different groups from aldonitrones. However, their odor ranges were found as animalic, medical, waxy, and ozonic undertones in common.en_US
dc.description.sponsorshipTUBITAK (Turkish Scientific and Technological Research Council) [119Z743]en_US
dc.identifier.citationSağırlı, A., Acar, H., Özçal, H. E., & Büyükbayram, M. (2022). Microwave-assisted synthesis and odor characteristics of some new isoxazolidines. Synthetic Communications, 52(21), 2067-2077.en_US
dc.identifier.doi10.1080/00397911.2022.2130079
dc.identifier.endpage2077en_US
dc.identifier.issn0039-7911
dc.identifier.issn1532-2432
dc.identifier.issue21en_US
dc.identifier.scopus2-s2.0-85139558864en_US
dc.identifier.scopusqualityQ3en_US
dc.identifier.startpage2067en_US
dc.identifier.urihttps://doi.org/10.1080/00397911.2022.2130079
dc.identifier.urihttps://hdl.handle.net/20.500.12491/11430
dc.identifier.volume52en_US
dc.identifier.wosWOS:000865377200001en_US
dc.identifier.wosqualityQ3en_US
dc.indekslendigikaynakWeb of Scienceen_US
dc.indekslendigikaynakScopusen_US
dc.institutionauthorSağırlı, Akın
dc.institutionauthorAcar, Havva
dc.institutionauthorÖzçal, Hakan Emre
dc.language.isoenen_US
dc.publisherTaylor & Francis Inc.en_US
dc.relation.ispartofSynthetic Communicationsen_US
dc.relation.publicationcategoryMakale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanıen_US
dc.relation.tubitakTÜBİTAK (Turkish Scientific and Technological Research Council) [119Z743]
dc.rightsinfo:eu-repo/semantics/closedAccessen_US
dc.subjectAldonitroneen_US
dc.subjectIsoxazolidineen_US
dc.subjectMethacrylate Esteren_US
dc.subjectMicrowave Heatingen_US
dc.subjectOdoren_US
dc.subjectInhibitionen_US
dc.titleMicrowave-assisted synthesis and odor characteristics of some new isoxazolidinesen_US
dc.typeArticleen_US

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