Effect of magnesium source on the fabrication of kotoite Mg3B2O6 ceramic

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dc.authorid0000-0002-7585-0136
dc.authorid0000-0003-1790-6143
dc.contributor.authorMorkan, Ayşe
dc.contributor.authorGül, Esra
dc.contributor.authorMorkan, İzzet
dc.contributor.authorKahveci, Gülden
dc.date.accessioned2021-06-23T19:49:24Z
dc.date.available2021-06-23T19:49:24Z
dc.date.issued2018
dc.departmentBAİBÜ, Fen Edebiyat Fakültesi, Kimya Bölümüen_US
dc.description.abstractThe effect of magnesium source on the fabrication of kotoite, Mg3B2O6, ceramic has been investigated by high temperature solid-state reaction route based on the calcination of different magnesium sources, containing magnesium oxide, magnesium carbonate, magnesium sulfate, and magnesium nitrate with boric acid. The X-ray powder diffraction results showed that single-phase kotoite, Mg3B2O6, was synthesized using MgNO3.6H(2)O and 5 wt.% excess of H3BO3 powders as starting materials at 900 degrees C for 48hours. Mg3B2O6 obtained, is well crystallized, in orhorhombic crystal structure with lattice parameters of a=5.399(9), b=8.424(6), and c=4.506(5) angstrom. Jana2006 refinement of this product shows excellent fit of the experimental data with software data, GOF= 1.33. The crystallite size of the product was calculated as 40.50nm using Debye-Scherrer's equation. The existence of BO3 triangles were detected by FTIR measurements of Mg3B2O6. The thermal properties were studied in the temperature range of 20 degrees C to 1400 degrees C by TG/DTA. The results showed that thermal stability of Mg3B2O6 is detected about 1380 degrees C. Scanning electron microscopy was employed for observation of microstructure. The microstucture of obtained ceramic samples strongly depended on the magnesium source on the fabrication of Mg3B2O6 ceramic.en_US
dc.identifier.doi10.1111/ijac.13024
dc.identifier.endpage1593en_US
dc.identifier.issn1546-542X
dc.identifier.issn1744-7402
dc.identifier.issue6en_US
dc.identifier.scopus2-s2.0-85054299906en_US
dc.identifier.scopusqualityQ2en_US
dc.identifier.startpage1584en_US
dc.identifier.urihttps://doi.org/10.1111/ijac.13024
dc.identifier.urihttps://hdl.handle.net/20.500.12491/9492
dc.identifier.volume15en_US
dc.identifier.wosWOS:000446324500028en_US
dc.identifier.wosqualityQ2en_US
dc.indekslendigikaynakWeb of Scienceen_US
dc.indekslendigikaynakScopusen_US
dc.institutionauthorMorkan, Ayşe
dc.institutionauthorGül, Esra
dc.institutionauthorMorkan, İzzet
dc.institutionauthorKahveci, Gülden
dc.language.isoenen_US
dc.publisherWileyen_US
dc.relation.ispartofInternational Journal Of Applied Ceramic Technologyen_US
dc.relation.publicationcategoryMakale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanıen_US
dc.rightsinfo:eu-repo/semantics/closedAccessen_US
dc.subjectBoratesen_US
dc.subjectKotoiteen_US
dc.subjectNanoparticlesen_US
dc.subjectSynthesisen_US
dc.subjectThermal Analysisen_US
dc.titleEffect of magnesium source on the fabrication of kotoite Mg3B2O6 ceramicen_US
dc.typeArticleen_US

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