Dopamine-imprinted monolithic column for capillary electrochromatography

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dc.authorid0000-0002-6672-6862en_US
dc.authorid0000-0003-3260-1639
dc.authorid0000-0003-0177-5134
dc.contributor.authorAşır, Süleyman
dc.contributor.authorSarı, Duygu
dc.contributor.authorDerazshamshir, Ali
dc.contributor.authorYılmaz, Fatma
dc.contributor.authorŞarkaya, Koray
dc.date.accessioned2021-06-23T19:45:10Z
dc.date.available2021-06-23T19:45:10Z
dc.date.issued2017
dc.departmentBAİBÜ, Gerede Meslek Yüksekokulu, Kimya Ve Kimyasal İşleme Teknolojileri Bölümüen_US
dc.description.abstractA dopamine-imprinted monolithic column was prepared and used in capillary electrochromatography as stationary phase for the first time. Dopamine was selectively separated from aqueous solution containing the competitor molecule norepinephrine, which is similar in size and shape to the template molecule. Morphology of the dopamine-imprinted column was observed by scanning electron microscopy. The influence of the organic solvent content of mobile phase, applied pressure and pH of the mobile phase on the recognition of dopamine by the imprinted monolithic column has been evaluated, and the imprinting effect in the dopamine-imprinted monolithic polymer was verified. Developed dopamine-imprinted monolithic column resulted in excellent separation of dopamine from structurally related competitor molecule, norepinephrine. Separation was achieved in a short period of 10 min, with the electrophoretic mobility of 5.81x10(-5)m(2)V(-1)s(-1) at pH 5.0 and 500mbar pressure.en_US
dc.identifier.doi10.1002/elps.201700228
dc.identifier.endpage3012en_US
dc.identifier.issn0173-0835
dc.identifier.issn1522-2683
dc.identifier.issue22-23en_US
dc.identifier.pmid28786521en_US
dc.identifier.scopus2-s2.0-85036501904en_US
dc.identifier.scopusqualityQ2en_US
dc.identifier.startpage3003en_US
dc.identifier.urihttps://doi.org/10.1002/elps.201700228
dc.identifier.urihttps://hdl.handle.net/20.500.12491/9110
dc.identifier.volume38en_US
dc.identifier.wosWOS:000416867300024en_US
dc.identifier.wosqualityQ2en_US
dc.indekslendigikaynakWeb of Scienceen_US
dc.indekslendigikaynakScopusen_US
dc.indekslendigikaynakPubMeden_US
dc.institutionauthorYılmaz, Fatma
dc.language.isoenen_US
dc.publisherWileyen_US
dc.relation.ispartofElectrophoresisen_US
dc.relation.publicationcategoryMakale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanıen_US
dc.rightsinfo:eu-repo/semantics/closedAccessen_US
dc.subjectCECen_US
dc.subjectDopaminen_US
dc.subjectMIPen_US
dc.subjectMonolithen_US
dc.titleDopamine-imprinted monolithic column for capillary electrochromatographyen_US
dc.typeArticleen_US

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