Development of Molecularly Imprinted Magnetic Amino Acid-Based Nanoparticles for Voltammetric Analysis of Lead Ions in Honey

dc.authoridGOKTURK, ILGIM/0000-0001-7292-7241
dc.authoridOzgoren, Murat/0000-0002-7984-2571
dc.authoridTURKMEN, DENIZ/0000-0003-0161-172X
dc.authoridAsir, Suleyman/0000-0002-6672-6862
dc.authoridKaragozlu, Mehmet/0000-0002-6737-6702
dc.contributor.authorKaragozlu, Mehmet
dc.contributor.authorAsir, Suleyman
dc.contributor.authorAbu Shama, Nemah
dc.contributor.authorGokturk, Ilgim
dc.contributor.authorYilmaz, Fatma
dc.contributor.authorTurkmen, Deniz
dc.contributor.authorDenizli, Adil
dc.date.accessioned2024-09-25T19:58:48Z
dc.date.available2024-09-25T19:58:48Z
dc.date.issued2024
dc.departmentAbant İzzet Baysal Üniversitesien_US
dc.description.abstractLead (Pb) is a hazardous metal that poses a significant threat to both the environment and human health. The presence of Pb in food products such as honey can pose a significant risk to human health and is therefore important to detect and monitor. In this study, we propose a voltammetric detection method using molecularly imprinted polymer (MIP) electrodes to detect Pb (II) ions in honey. Pb (II) ion-imprinted amino acid-based nanoparticles with magnetic properties on a carbon paste electrode (MIP-CPE) were designed to have high sensitivity and selectivity towards Pb (II) ions in the honey sample. Zetasizer measurements, electron spin resonance, and scanning electron microscopy were used to characterize magnetic polymeric nanoparticles. The results showed that the voltammetric detection method using MIP-CPE was able to accurately detect Pb (II) ions in honey samples with a low detection limit. The proposed method offers a simple, rapid, cost-effective solution for detecting Pb (II) ions in honey. It could potentially be applied to other food products to ensure their safety for human consumption. The MIP-CPE sensor was designed to have high sensitivity and selectivity towards Pb (II) ions in the honey sample. The results showed that the technique was able to deliver highly sensitive results since seven different concentrations were prepared and detected to obtain an R2 of 0.9954, in addition to a low detection limit (LOD) of 0.0912 mu M and a low quantification limit (LOQ) of 0.276 mu M. Importantly, the analysis revealed no trace of Pb (II) ions in the honey samples obtained from Cyprus.en_US
dc.identifier.doi10.3390/polym16131782
dc.identifier.issn2073-4360
dc.identifier.issue13en_US
dc.identifier.pmid39000638en_US
dc.identifier.scopus2-s2.0-85198442180en_US
dc.identifier.scopusqualityQ1en_US
dc.identifier.urihttps://doi.org/10.3390/polym16131782
dc.identifier.urihttps://hdl.handle.net/20.500.12491/13753
dc.identifier.volume16en_US
dc.identifier.wosWOS:001269722900001en_US
dc.identifier.wosqualityN/Aen_US
dc.indekslendigikaynakWeb of Scienceen_US
dc.indekslendigikaynakScopusen_US
dc.indekslendigikaynakPubMeden_US
dc.institutionauthorOzgoren, Murat
dc.language.isoenen_US
dc.publisherMdpien_US
dc.relation.ispartofPolymersen_US
dc.relation.publicationcategoryMakale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanıen_US
dc.rightsinfo:eu-repo/semantics/openAccessen_US
dc.snmzYK_20240925en_US
dc.subjectleaden_US
dc.subjectimprinted polymeren_US
dc.subjectmagnetic nanoparticlesen_US
dc.subjectcarbon paste electrodeen_US
dc.subjectelectrochemical biosensoren_US
dc.subjectdifferential pulse voltammetryen_US
dc.subjecthoneyen_US
dc.titleDevelopment of Molecularly Imprinted Magnetic Amino Acid-Based Nanoparticles for Voltammetric Analysis of Lead Ions in Honeyen_US
dc.typeArticleen_US

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