Novel benzothiophene 1,1-dioxide deoxygenation path for the microwave-assisted synthesis of substituted benzothiophene-fused pyrrole derivatives

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dc.authorid0000-0002-0873-694Xen_US
dc.authorid0000-0003-2739-7725
dc.contributor.authorKarakuş, Hamza
dc.contributor.authorDürüst, Yaşar
dc.date.accessioned2021-06-23T19:48:59Z
dc.date.available2021-06-23T19:48:59Z
dc.date.issued2017
dc.departmentBAİBÜ, Fen Edebiyat Fakültesi, Kimya Bölümüen_US
dc.description.abstractThe reaction of C-(4-substituted-phenyl)-N-(benzoyl)-N-methylglycines with benzo[b]thiophene 1,1-dioxide unexpectedly gave benzothiophene-fused pyrrole derivatives in toluene under microwave irradiation via a cycloaddition and metal-free Pummerer-type sulfone deoxygenation path. In order to obtain the desired sulfone derivatives, the sulfide group underwent oxidation with m-CPBA to afford sulfones. The structures of all the new products were elucidated by spectroscopic/physical methods and, in two cases, by X-ray diffraction. [GRAPHICS]en_US
dc.identifier.doi10.1007/s11030-016-9700-0
dc.identifier.endpage60en_US
dc.identifier.issn1381-1991
dc.identifier.issn1573-501X
dc.identifier.issue1en_US
dc.identifier.pmid27677736en_US
dc.identifier.scopus2-s2.0-84988735453en_US
dc.identifier.scopusqualityQ2en_US
dc.identifier.startpage53en_US
dc.identifier.urihttps://doi.org/10.1007/s11030-016-9700-0
dc.identifier.urihttps://hdl.handle.net/20.500.12491/9301
dc.identifier.volume21en_US
dc.identifier.wosWOS:000394440900005en_US
dc.identifier.wosqualityQ2en_US
dc.indekslendigikaynakWeb of Scienceen_US
dc.indekslendigikaynakScopusen_US
dc.indekslendigikaynakPubMeden_US
dc.institutionauthorKarakuş, Hamza
dc.institutionauthorDürüst, Yaşar
dc.language.isoenen_US
dc.publisherSpringeren_US
dc.relation.ispartofMolecular Diversityen_US
dc.relation.publicationcategoryMakale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanıen_US
dc.rightsinfo:eu-repo/semantics/closedAccessen_US
dc.subjectCycloadditionen_US
dc.subjectSulfone Deoxygenationen_US
dc.subjectBenzothiopheneen_US
dc.subjectPyrroleen_US
dc.subjectMicrowave synthesisen_US
dc.subjectHeterocyclizationen_US
dc.titleNovel benzothiophene 1,1-dioxide deoxygenation path for the microwave-assisted synthesis of substituted benzothiophene-fused pyrrole derivativesen_US
dc.typeArticleen_US

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