Simultaneous preconcentration and determination of Cu(II), Ni(II), and Co(II) in food and environmental samples by the application of chelate adsorption on amberlite XAD-1180

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dc.authorid0000-0002-0374-3921en_US
dc.authorid0000-0002-5619-3388en_US
dc.contributor.authorTopuz, Berrin
dc.contributor.authorAltınışık, Ece Talya
dc.date.accessioned2023-07-26T11:01:22Z
dc.date.available2023-07-26T11:01:22Z
dc.date.issued2023en_US
dc.departmentBAİBÜ, Mühendislik Fakültesi, Çevre Mühendisliği Bölümüen_US
dc.descriptionScientific Research Projects Unit of Abant Izzet Baysal University(Abant Izzet Baysal University)en_US
dc.description.abstractA simultaneous preconcentration and determination procedure for solid phase extraction on AXAD-1180 as 2,6-dimethylmorpholinedithiocarbamate (DMMDTC) chelates and spectrophotometric determinations of Cu (II), Ni (II), and Co (II) in food and environmental samples is proposed in the present work. The effect of some SPE parameters, such as reagent amount, sample pH, eluent type, concentration, and volume, sample and eluent flow rate, and sample volume, on trace metal ion recovery (R%) for the method developed in the standard model solution medium was investigated. Cu(II), Ni(II), and Co(II) retained as DMMDTC complexes on Amberlite XAD-1180 were eluted with 10 mL of 1 M HNO3 (in acetone). Foreign ions were also studied individually on the recovery of trace metal ions using the developed method. Cu(II), Ni(II), and Co(II) ions were preconcentrated and separated from the sample using the developed SPE method, and their concentrations were simultaneously determined using the UV-Vis spectrophotometric method. The spectrophotometric determination was made by measuring the absorbance of colored chelates of metal ions complexed with DMMDTC in a surfactant medium (1% Triton X-100) at wavelengths of 460, 328, and 342 nm for Cu(II), Ni(II), and Co(II), respectively. To test the method's accuracy, certified reference materials (CRM 1204 waste water and TMDA-70.2 Ontario lake water) were analyzed using the proposed method, and metal recoveries were calculated to be between 97.1 and 100.7%. The proposed method worked well with the wheat flour sample. Wheat flour has Cu(II) and Ni(II) contents of 2.16 mu gmL(-1) and 0.56 mu gmL(-1), respectively.en_US
dc.description.sponsorshipScientific Research Projects Unit of Abant Izzet Baysal University [2018.09.04.1379]en_US
dc.identifier.citationTopuz, B., & Altinişik, E. T. (2023). Simultaneous preconcentration and determination of Cu (II), Ni (II), and Co (II) in food and environmental samples by the application of chelate adsorption on Amberlite XAD-1180. Food Analytical Methods, 1-12.en_US
dc.identifier.doi10.1007/s12161-023-02476-7
dc.identifier.endpage1054en_US
dc.identifier.issn1936-9751
dc.identifier.issn1936-976X
dc.identifier.issue6en_US
dc.identifier.scopus2-s2.0-85151541499en_US
dc.identifier.scopusqualityQ2en_US
dc.identifier.startpage1043en_US
dc.identifier.urihttp://dx.doi.org/10.1007/s12161-023-02476-7
dc.identifier.urihttps://hdl.handle.net/20.500.12491/11362
dc.identifier.volume16en_US
dc.identifier.wosWOS:000964430700002en_US
dc.identifier.wosqualityQ2en_US
dc.indekslendigikaynakWeb of Scienceen_US
dc.indekslendigikaynakScopusen_US
dc.institutionauthorTopuz, Berrin
dc.language.isoenen_US
dc.publisherSpringeren_US
dc.relation.ispartofFood Analytical Methodsen_US
dc.relation.publicationcategoryMakale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanıen_US
dc.rightsinfo:eu-repo/semantics/openAccessen_US
dc.subjectSolid-Phase Extractionen_US
dc.subjectAmberlite XAD-1180en_US
dc.subject6-Dimethylmorpholinedithiocarbamateen_US
dc.subjectAtomic-Absorption-Spectrometryen_US
dc.subjectCloud-Point Extractionen_US
dc.subjectHeavy-Metalsen_US
dc.titleSimultaneous preconcentration and determination of Cu(II), Ni(II), and Co(II) in food and environmental samples by the application of chelate adsorption on amberlite XAD-1180en_US
dc.typeArticleen_US

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