Synthesis and spectroscopic characterization of group 6 pentacarbonyl(4-substituted pyridine)metal(0) complexes

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dc.authorid0000-0002-6302-1429en_US
dc.authorid0000-0001-9036-5836en_US
dc.authorid0000-0002-7585-0136
dc.contributor.authorTuç, Çiğdem
dc.contributor.authorMorkan, İzzet Amour
dc.contributor.authorÖzkar, Saim
dc.date.accessioned2021-06-23T19:19:59Z
dc.date.available2021-06-23T19:19:59Z
dc.date.issued2007
dc.departmentBAİBÜ, Fen Edebiyat Fakültesi, Kimya Bölümüen_US
dc.description.abstractCarbonyl-metal (M:Cr, Mo, W) derivatives of 4-substituted pyridines [4-methylpyridine (4-mp), 4-tert-butylpyridine (4-tbp) and 4-dimethylaminopyridine (4-dmap)] where the metal center is bonded to the nitrogen atom of the substituted pyridine ring are described. The organometallic complexes, M(CO)(5)L, were synthesized by either the direct reaction of the metal hexacarbonyls or by the thermal substitution of M(CO)(5)(THF) with the pyridine ligands; 4-methylpyridine (1), 4-tert-butylpyridine (2), 4-dimethylaminopyridine (3). The reported complexes were purified by column chromatography and recrystallization. The complexes were all characterized in solution by elemental analysis, MS, ir ,(1) H-nmr and (13) stopC-nmr spectroscopies.en_US
dc.identifier.doi10.1007/s11243-007-0239-x
dc.identifier.endpage731en_US
dc.identifier.issn0340-4285
dc.identifier.issn1572-901X
dc.identifier.issue6en_US
dc.identifier.scopus2-s2.0-34547610226en_US
dc.identifier.scopusqualityQ2en_US
dc.identifier.startpage727en_US
dc.identifier.urihttps://doi.org/10.1007/s11243-007-0239-x
dc.identifier.urihttps://hdl.handle.net/20.500.12491/6038
dc.identifier.volume32en_US
dc.identifier.wosWOS:000248624300007en_US
dc.identifier.wosqualityQ3en_US
dc.indekslendigikaynakWeb of Scienceen_US
dc.indekslendigikaynakScopusen_US
dc.institutionauthorTuç, Çiğdem
dc.institutionauthorMorkan, İzzet Amour
dc.language.isoenen_US
dc.publisherSpringeren_US
dc.relation.ispartofTransition Metal Chemistryen_US
dc.relation.publicationcategoryMakale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanıen_US
dc.rightsinfo:eu-repo/semantics/closedAccessen_US
dc.subject6 Pentacarbonyl Complexesen_US
dc.titleSynthesis and spectroscopic characterization of group 6 pentacarbonyl(4-substituted pyridine)metal(0) complexesen_US
dc.typeArticleen_US

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