The synthesis of sodium sulfide pentahydrate, Na2S.5H(2)O, through a solid-gas reaction of sulfidizing gas mixture with sodium carbonate, Na2CO3

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dc.authorid0000-0001-5931-829X
dc.authorid0000-0001-7301-4698
dc.authorid0000-0002-7585-0136
dc.authorid0000-0003-2283-9512
dc.contributor.authorGüler, Halil
dc.contributor.authorKurtuluş, Figen
dc.contributor.authorKadan, İmdat
dc.contributor.authorMorkan, Ayşe
dc.contributor.authorAkın, Sebahat
dc.date.accessioned2021-06-23T19:19:10Z
dc.date.available2021-06-23T19:19:10Z
dc.date.issued2006
dc.departmentBAİBÜ, Fen Edebiyat Fakültesi, Kimya Bölümüen_US
dc.description.abstractIn this study, the sulfidization of Na2CO3 was investigated by using a solid-gas reaction under a sulfidizing gas mixture, which consisted of COS, CS2, and S-2 gases. Sodium sulfide pentahydrate, Na2S center dot 5H(2)O, was prepared from sodium carbonate, Na2CO3, via a sulfidizing gas mixture by a solid-gas reaction under the cooling of a nitrogen atmosphere. The observed phase was found to be the pentahydrated form of sodium sulfide. This crystalline form was determined by X-ray powder diffraction (XRD) technique. Since sodium sulfide is strongly hygroscopic, the pentahydrated crystalline form was observed in XRD measurements for all repeated experiments. The crystal unit cell parameters of the synthesized product were in excellent agreement with values given in the JCPDS card number 18-1249. The sodium sulfide pentahydrate has an orthorhombic crystal structure with the unit cell parameters of a = 6.475, b = 12.55, C = 8.655 angstrom, space group, Cmcm and Z = 4.en_US
dc.identifier.doi10.1080/10426500500327063
dc.identifier.endpage1379en_US
dc.identifier.issn1042-6507
dc.identifier.issn1563-5325
dc.identifier.issue6en_US
dc.identifier.scopus2-s2.0-33646457965en_US
dc.identifier.scopusqualityQ4en_US
dc.identifier.startpage1371en_US
dc.identifier.urihttps://doi.org/10.1080/10426500500327063
dc.identifier.urihttps://hdl.handle.net/20.500.12491/5888
dc.identifier.volume181en_US
dc.identifier.wosWOS:000237605500015en_US
dc.identifier.wosqualityQ4en_US
dc.indekslendigikaynakWeb of Scienceen_US
dc.indekslendigikaynakScopusen_US
dc.institutionauthorMorkan, Ayşe
dc.language.isoenen_US
dc.publisherTaylor & Francis Ltden_US
dc.relation.ispartofPhosphorus Sulfur And Silicon And The Related Elementsen_US
dc.relation.publicationcategoryMakale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanıen_US
dc.rightsinfo:eu-repo/semantics/closedAccessen_US
dc.subjectSodium Sulfide Pentahydrateen_US
dc.subjectSolid-gas Reactionsen_US
dc.subjectSynthesisen_US
dc.subjectX-ray Powder Diffractionen_US
dc.titleThe synthesis of sodium sulfide pentahydrate, Na2S.5H(2)O, through a solid-gas reaction of sulfidizing gas mixture with sodium carbonate, Na2CO3en_US
dc.typeArticleen_US

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