Metal contamination in fruit juices in Turkey : method validation and uncertainty budget

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dc.authorid0000-0003-1174-0197en_US
dc.authorid0000-0002-4940-1839en_US
dc.authorid0000-0002-0107-0110
dc.contributor.authorKılıç, Serpil
dc.contributor.authorKarakaş, Serpil Yenisoy
dc.contributor.authorKılıç, Murat
dc.date.accessioned2021-06-23T19:37:29Z
dc.date.available2021-06-23T19:37:29Z
dc.date.issued2015
dc.departmentBAİBÜ, Fen Edebiyat Fakültesi, Kimya Bölümüen_US
dc.description.abstractThe consumption rate of fruit juices has rapidly increased in the past years. In this study, the detailed discussion of method validation and uncertainty calculations and then the evaluation of concentrations of Ag, As, Be, Bi, Cd, Co, Pb, Se, and V determined in 42 commercial fruit juice samples by using inductively coupled plasma mass spectrometry (ICP-MS) were presented. The samples were digested with nitric acid and hydrogen peroxide in a microwave oven. In order to verify the recovery of the proposed method, standard reference material was used. The recovery values changed between 83 and 118 %. The average precision values for all elements were determined as the relative standard deviation RSD (%) in the range of 1.3 and 2.9 %. Applying the bottom-up method, it was found that the main contributions to the combined uncertainty came from the calibration curve and the method recovery. The concentrations of all metals did not exceed the international and Turkish codex values.en_US
dc.identifier.doi10.1007/s12161-015-0136-4
dc.identifier.endpage2495en_US
dc.identifier.issn1936-9751
dc.identifier.issn1936-976X
dc.identifier.issue10en_US
dc.identifier.scopus2-s2.0-84942504425en_US
dc.identifier.scopusqualityQ2en_US
dc.identifier.startpage2487en_US
dc.identifier.urihttps://doi.org/10.1007/s12161-015-0136-4
dc.identifier.urihttps://hdl.handle.net/20.500.12491/8166
dc.identifier.volume8en_US
dc.identifier.wosWOS:000361985500010en_US
dc.identifier.wosqualityQ2en_US
dc.indekslendigikaynakWeb of Scienceen_US
dc.indekslendigikaynakScopusen_US
dc.institutionauthorKarakaş, Serpil Yenisoy
dc.language.isoenen_US
dc.publisherSpringeren_US
dc.relation.ispartofFood Analytical Methodsen_US
dc.relation.publicationcategoryMakale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanıen_US
dc.rightsinfo:eu-repo/semantics/closedAccessen_US
dc.subjectFruit Juicesen_US
dc.subjectHeavy Metalsen_US
dc.subjectContaminationen_US
dc.subjectInductively Coupled Plasma Mass Spectrometryen_US
dc.subjectMethod Validationen_US
dc.subjectUncertainty Budgeten_US
dc.titleMetal contamination in fruit juices in Turkey : method validation and uncertainty budgeten_US
dc.typeArticleen_US

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