Some reactions of 2-(4-substitutedphenyl)-2-(n-methyl-n-4-substitutedbenzamido) acetic acids

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dc.authorid0000-0002-8658-3897en_US
dc.authorid0000-0002-8658-3897en_US
dc.authorid0000-0002-0873-694Xen_US
dc.contributor.authorDürüst, Yaşar
dc.contributor.authorKarakuş, Hamza
dc.contributor.authorKariuki, Benson M.
dc.contributor.authorKnight, David W.
dc.date.accessioned2021-06-23T19:50:09Z
dc.date.available2021-06-23T19:50:09Z
dc.date.issued2018
dc.departmentBAİBÜ, Fen Edebiyat Fakültesi, Kimya Bölümüen_US
dc.description.abstractIn situ generated 2,4-diaryl substituted munchnones from 2-(4-substitutedphenyl)-2-(N-methyl-N-4-substitutedbenzamido)acetic acids react with acetic anhydride in the presence of 2-nitromethylene thiazolidine, which is most likely acting as a base, and unexpectedly undergo a Dakin-West type reaction and a concurrent autoxidation reaction leading to the formation of (E)-1-(N,4-dimethylbenzamido)-1-(4-fluorophenyl)prop-1-en-2-yl acetate, 4-substitutedphenyl-N-methyl-N-(4-substitutedbenzoyl) benzamides and p-substituted benzoic acids. In addition, a novel and efficient access to N-acyl urea derivatives is described by the reaction between 2-(4-substitutedphenyl)-2-(N-methyl-N-4-substitutedbenzamido)acetic acids and cyclohexyl, isopropyl carbodiimides in the presence of a base. The structures of all new products were identified on the basis of NMR and IR spectra, along with X-ray diffraction data and HRMS measurements. [GRAPHICS] .en_US
dc.identifier.doi10.1080/00397911.2018.1489966
dc.identifier.endpage2220en_US
dc.identifier.issn0039-7911
dc.identifier.issn1532-2432
dc.identifier.issue17en_US
dc.identifier.scopus2-s2.0-85049630573en_US
dc.identifier.scopusqualityQ3en_US
dc.identifier.startpage2206en_US
dc.identifier.urihttps://doi.org/10.1080/00397911.2018.1489966
dc.identifier.urihttps://hdl.handle.net/20.500.12491/9716
dc.identifier.volume48en_US
dc.identifier.wosWOS:000443914600008en_US
dc.identifier.wosqualityQ3en_US
dc.indekslendigikaynakWeb of Scienceen_US
dc.indekslendigikaynakScopusen_US
dc.institutionauthorDürüst, Yaşar
dc.institutionauthorKarakuş, Hamza
dc.language.isoenen_US
dc.publisherTaylor & Francis Incen_US
dc.relation.ispartofSynthetic Communicationsen_US
dc.relation.publicationcategoryMakale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanıen_US
dc.rightsinfo:eu-repo/semantics/openAccessen_US
dc.subjectAcyl Ureaen_US
dc.subjectDakin-West Reactionen_US
dc.subjectMunchnone Precursoren_US
dc.subjectNitromethylene Thiazolidineen_US
dc.titleSome reactions of 2-(4-substitutedphenyl)-2-(n-methyl-n-4-substitutedbenzamido) acetic acidsen_US
dc.typeArticleen_US

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