New Synthetic Methodology for Construction of the 1,3,4,5-Tetrahydro-2H-1,3-benzodiazepin-2-one Skeleton

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dc.authorid0000-0002-8238-6941en_US
dc.authorid0000-0002-6311-8917
dc.contributor.authorDengiz, Çağatay
dc.contributor.authorÖzcan, Sevil
dc.contributor.authorŞahin, Ertan
dc.contributor.authorBalcı, Metin
dc.date.accessioned2021-06-23T19:27:06Z
dc.date.available2021-06-23T19:27:06Z
dc.date.issued2010
dc.departmentBAİBÜ, Fen Edebiyat Fakültesi, Kimya Bölümüen_US
dc.description.abstractWe hereby report a new synthetic methodology for construction of the 1,3,4,5-tetrahydro-2H-1,3-benzodiazepin-2-one skeleton. 2-(2-Carboxyethyl)benzoic acid was converted into the corresponding bis(acyl azide). Curtius rearrangement of the diazide followed by reaction with alcohols provided diurethane derivatives. Ring-closure reaction of the diurethanes with base resulted in formation of the 1,3-benzodiazepin-2-one skeleton.en_US
dc.identifier.doi10.1055/s-0029-1218673
dc.identifier.endpage1370en_US
dc.identifier.issn0039-7881
dc.identifier.issn1437-210X
dc.identifier.issue8en_US
dc.identifier.scopus2-s2.0-77950536239en_US
dc.identifier.scopusqualityQ1en_US
dc.identifier.startpage1365en_US
dc.identifier.urihttps://doi.org/10.1055/s-0029-1218673
dc.identifier.urihttps://hdl.handle.net/20.500.12491/6737
dc.identifier.wosWOS:000277767800016en_US
dc.identifier.wosqualityQ2en_US
dc.indekslendigikaynakWeb of Scienceen_US
dc.indekslendigikaynakScopusen_US
dc.institutionauthorÖzcan, Sevil
dc.language.isoenen_US
dc.publisherGeorg Thieme Verlag Kgen_US
dc.relation.ispartofSynthesis-Stuttgarten_US
dc.relation.publicationcategoryMakale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanıen_US
dc.rightsinfo:eu-repo/semantics/closedAccessen_US
dc.subjectAcyl Azideen_US
dc.subjectIsocyanateen_US
dc.subjectCurtius Rearrangementen_US
dc.subjectUrethanesen_US
dc.subjectBenzodiazepinoneen_US
dc.titleNew Synthetic Methodology for Construction of the 1,3,4,5-Tetrahydro-2H-1,3-benzodiazepin-2-one Skeletonen_US
dc.typeArticleen_US

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WoS İndeksli Yayınlar Koleksiyonu
Kimya Bölümü Koleksiyonu
Scopus İndeksli Yayınlar Koleksiyonu