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Öğe Synthesis of iPF(2 alpha)-V: a new route(Pergamon-Elsevier Science Ltd, 1999) Hwang, Seong Woo; Adıyaman, Mustafa; Lawson, John A.; FitzGerald, Garret A.; Rokach, JoshuaWe are reporting here on a new synthesis of iPF(2 alpha)-V, and we also disclose the first report on the synthesis of 12-epi-iPF(2 alpha)-V. The new total synthesis of iPF(2 alpha)-V reported here is designed to address metabolism and analytical issues. We have used this new route and also performed the total synthesis of 17,17,18,18-tetradeutero-iPF(2 alpha)-V. The availability of the deuterated analog of iPF(2 alpha)-V is the first step in our attempt to quantitate this isoprostane in biological fluids by GC and LC-MS.
